THE MINERAL WATER TESTS METHODS METROLOGICAL ANALYSIS AND THE PROPOSALS ON THEIR IMPLEMENTATION IN UKRAINE

  • A. Yu. Kysylevska Odessa National Polytechnic University. 65044, Ukraine, Odessa, Shevchenko av., 1
  • K. D. Babov State Institution «Ukrainian Research Institute of Medical Rehabilitation and Balneology of the Ministry of Health of Ukraine», 65014, Odesa, Lermontovsky, 6
  • I. V. Prokopovich Odessa National Polytechnic University. 65044, Ukraine, Odessa, Shevchenko av., 1
  • Ch. A Koeva State Institution «Ukrainian Research Institute of Medical Rehabilitation and Balneology of the Ministry of Health of Ukraine», 65014, Odesa, Lermontovsky, 6
Keywords: mineral waters, test methods, metrological characteristics, validation, standard.

Abstract

In connection with the necessity to unify the procedures and requirements applicable to goods and services, first of all, with regard to conformity assessment, in order to eliminate technical barriers to trade, a list of methods for testing mineral waters has been analyzed, according to which their assessment of conformity and determination of individual safety and quality indicators. The paper analyzes the metrological characteristics of the methods approved in the form of international, national standards, standards adopted before 1992, test methods for assessing their suitability for implementation not only in the testing, but also in the production laboratories. According to the results of the analysis of 42 indicators of the measurement methodology, which are specified in DSTU 878-93 (regulatory document on packaged mineral water) and GSTU 42.10-02-96 (normative document on medical waters used in sanatorium practice), 13 indicators , which are mandatory, as they are specified in the relevant normative documents, are not valid. According to the results of the analysis of the metrological characteristics of the methods of testing the indicators of safety and quality of mineral waters, a list of methods of tests of mineral waters for the period 2019-2021 has been developed, which includes national standards certified in Ukraine methodology and GOST for drinking water, in particular, on sulfates, ammonium and iron . However, the effect of these GOST on the testing of drinking water after 2021 will be abolished, and they should also be replaced either internationally or to develop national standards. In selecting the methods of testing mineral waters, two aspects were taken into account: the conformity of metrological characteristics of the methods during the assessment of the conformity of mineral waters, taking into account the features of the composition of the mineral water itself (applicability of the method for both low and high mineral waters), and the economic feasibility of testing for the appropriate method (due to the impossibility of many testing and production laboratories to use high-value equipment). In order to provide modern standards (international and national) of packaged mineral water producers and test laboratories conducting an assessment of the conformity of mineral waters, a list of methods for testing mineral waters, which is to be developed in Ukraine for the replacement of interstate GOST or methods, the metrological characteristics of which do not correspond to the current one, is proposed. in Ukraine the rules of legal metrology, and to give them the status of national standards (for the definition of Pseudomonas spit, sulfates, ammonium, bro copper and iodide). This will enable Ukrainian producers of packaged mineral water to optimize production costs for the production of Ukrainian products and successfully expand its share in the foreign market.

Downloads

Download data is not yet available.

References

Mahinova, A. / A. Mahinova, V. Mykulyak // Morskoe pravo ot 28/04/15 (Tema nomera: Morskoe pravo barernaya lestnica). −[Elektronnij resurs]. — Rezhim dostupu: www.sk.ua/sites/default/files/barernaya_lestnic a_--_yuridicheskaya_ praktika.pdf

Pro osnovni principi ta vimogi do bezpechnosti ta yakosti harchovih produktiv: Zakon Ukrayini v relakciyi Zakonu vid 22.07.2014 r. № 1602-VII // Vidomosti Verhovnoyi Radi Ukrayini – 1998. – № 19. – P. 98.

Pro zatverdzhennya Programi diyalnosti Kabinetu Ministriv Ukrayini: Postanova Kabinetu Ministriv Ukrayini vid 09.12.2014 r. № 695. −[Elektronnij resurs]. — Rezhim dostupu: https://zakon.rada.gov.ua/laws/show/695-2014- %D0%BF

Vodi mineralni likuvalni. Tehnichni umovi: GSTU 42.10-02-96. − [Chinnij vid 1996- 06-24] — K.: Ministerstvo ohoroni zdorov’ya Ukrayini, 1996. — 30 p. — (Galuzevij standart Ukrayini).

Zakon Ukrayini «Pro metrologiyu ta metrologichnu diyalnist» // Vidomosti Verhovnoyi Radi (VVR), – 2014. – № 30. – P .1008.

Volodarskij V.Ye. Metrologichne zabezpechennya vimiryuvan i kontrolyu: navchalnij posibnik / Volodarskij Ye. T., Kuharchuk V.V., Podzharenko V.O., Serdyuk G.B. − Vinnicya: VDTU, 2001. – 219 p.

Bubela, T. Z. Fiziko-himichni vimiryuvannya. ― Lviv: Vid-vo NU «Lvivska politehnika», 2005. – 150 p.

Vyiyavlenie i identifikatsiya P. aeruginosa v ob'ektah okruzhayuschey sredyi (pischevyih produktah, vode, stochnyih zhidkostyah): metodicheskie rekomendatsii, utv. prikazom Nachalnika Glavnogo upravleniya karantinnyih ISSN 1993-9981 print ISSN 2415-3575 online Metodi ta priladi kontrolyu yakostI No 1 (42) 2019 95 infektsiy Minzdrava SSSR V. P.Sergieva ot 24.05.1984 g.

Reznikov, A. A. Metodi analizu prirodnih vod / A.A. Reznikiv Mulikovskaya E. P., Sokolov I. Yu. – M.: Nedra, 1970 p. – 488 s. 10. Metodika opredeleniya obshego organicheskogo ugleroda v prirodnyh minealnyh vodah: avtorskoe svidetelstvo № 1513398 vid 21.06.88 r. – Odessa: Ukrainskij nauchnoissledovatelskij mnstitut me8.

Metodika opredeleniya obschego organicheskogo ugleroda v prirodnyih minealnyih vodah: avtorskoe svidetelstvo # 1513398 vId 21.06.88 r. – Odessa: Ukrainskiy nauchno-issledovatelskiy mnstitut meditsinskoy reabilitatsii i kurortologii, 1988 g. – 7 s.

Metodika ekspressnogo opredeleniya ob'emnoy i udelnoy aktivnosti betaizluchayuschih nuklidov v vode, produktah pitaniya, rastitelnosti i pochve metodom «pryamogo» izmereniya «tolstyih» prob: prikaz Glavnogo sanitarnogo vracha Glavnogo sanitarno-profilakticheskogo upravleniya Minzdrava SSSR ot 12.08.86 r. P 123.

Metod lyuminestsentnogo opredeleniya urana: protokol zasedaniya Uchenogo soveta Ukrainskogo nauchno-issledovatelskogo instituta meditsinskoy reabilitatsii i kurortologii ot 03.10.1987 g. # 8. – Odessa: Ukrainskiy nauchnoissledovatelskiy mnstitut meditsinskoy reabilitatsii i kurortologii, 1988 g. – 8 p.

Posibnik z metodiv kontrolyu prirodnih mineralnih vod, shtuchno-mineralizovanih vod ta napoyiv na yih osnovi. Ch. 2. Mikrobiologichni doslidzhennya / Nikolenko S.I., Gluhovska S.M., Hmyelyevska O.M., Petrovska V.B. – MOZ Ukrayini; UkrNDIMRtaK. – Kiyiv: KIM, 2011.− 52 p.

Nikipelova, O.M. Posibnik z metodiv kontrolyu prirodnih mineralnih vod, shtuchnomineralizovanih vod ta napoyiv na yih osnovi. Ch.1. Fiziko-himichni doslidzhennya / MOZ Ukrayini, UkrNDIMRtaK / Nikipelova O.M., Filipenko T.G., Solodova L.B. — Odesa: Specializovane vid-vo «YuNESKO-SOCIO», 2002. — 96 p. — ISBN 966-7251-15-2.

Nastanova Eurachem «Pridatnist analitichnih metodiv dlya konkretnogo zastosuvannya. Nastanova dlya laboratorij z validaciyi metodiv ta sumizhnih pitan»: za red. B. Magnussona ta U. Ernemarka: pereklad drugogo vidannya 2014 r. – K.: TOV «Yurka Lyubchenka», 2016. − 92 p.

Published
2019-06-27
How to Cite
Kysylevska, A. Y., Babov, K. D., Prokopovich, I. V., & Koeva, C. A. (2019). THE MINERAL WATER TESTS METHODS METROLOGICAL ANALYSIS AND THE PROPOSALS ON THEIR IMPLEMENTATION IN UKRAINE. METHODS AND DEVICES OF QUALITY CONTROL, (1(42), 85-96. https://doi.org/10.31471/1993-9981-2019-1(42)-85-96
Section
METHODS AND DEVICES OF CONTROL OF TECHNOLOGICAL PARAMETERS